HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Trifluoromethyl)benzoic acid → 6-(4-trifluoromethylbenzoyl)amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Trifluoromethyl)benzoic acid | HCID 9966 | — |
| Reactant | 6-amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole | HCID 22611560 | — |
| Product | 6-(4-trifluoromethylbenzoyl)amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole | HCID 53872633 | 35.5% |
Reaction Steps
Beginning with 9.2 mg (0.040 mMol) 6-amino-3-(dimethyl)amino-1,2,3,4-tetrahydro-9H-carbazole and 19.2 mg (0.101 mMol) 4-trifluoromethylbenzoic acid, 5.7 mg (35%) of the title compound were recovered as a beige solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05814653 |
| Source dataset | uspto-grants-1998_09 |
| ORD ID | ord-2b3ef3fb217d41bc90a5e02f048c15a5 |
| Source note | uspto-grants-1998_09 |