HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-methyl-N-phenyl-hydrazine → 5-cyclopentyl-N'-methyl-N'-phenyl-6-(2,2,2-trifluoroethoxy)-3-pyridinecarboxylic acid hydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-methyl-N-phenyl-hydrazine | HCID 36299 | — |
| Reactant | 5-Cyclopentyl-6-(2,2,2-trifluoroethoxy)-3-pyridinecarboxylic acid | HCID 71294186 | — |
| Product | 5-cyclopentyl-N'-methyl-N'-phenyl-6-(2,2,2-trifluoroethoxy)-3-pyridinecarboxylic acid hydrazide | HCID 71294058 | — |
Reaction Steps
The title compound was synthesized in analogy to Example 1 using 5-cyclopentyl-6-(2,2,2-trifluoro-ethoxy)-3-pyridinecarboxylic acid (example 14c) and 1-methyl-1-phenyl-hydrazine (CAN 618-40-6) as starting materials; LC-MS (UV peak area/ESI) 98.0%, 394.1737 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08648099B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-196e0bc19b5941eb8d3a2be5fcd72ade |
| Source note | uspto-grants-2014_02 |