HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyaniline → 4-methoxy-N-(2-methoxyphenyl)benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyaniline | HCID 7000 | — |
| Reactant | 4-Methoxybenzenesulfonyl chloride | HCID 7401 | — |
| Product | 4-methoxy-N-(2-methoxyphenyl)benzenesulfonamide | HCID 743417 | 90.1% |
Reaction Steps
Using o-anisidine (1.0 ml, 8.55 mmol) and 4-methoxybenzenesulfonyl chloride (1.78 g, 8.55 mmol), the procedure of Reference Example 2 was repeated to obtain 2.26 g (90.1%) of the title compound in the form of colorless powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05728835 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-80f67fcb3ee14ef2b196db2ad72d47b4 |
| Source note | uspto-grants-1998_03 |