HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyaniline → 4-fluoro-N-(2-methoxyphenyl)benzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyaniline | HCID 7000 | — |
| Reactant | 4-Fluorobenzenesulfonyl chloride | HCID 9588 | — |
| Product | 4-fluoro-N-(2-methoxyphenyl)benzenesulfonamide | HCID 711079 | 93.1% |
Reaction Steps
Using o-anisidine (1.0 ml, 8.55 mmol) and 4-fluorobenzenesulfonyl chloride (1.7 g, 8.55 mmol), the procedure of Reference Example 2 was repeated to obtain 2.24 g (93.1%) of the title compound in the form of colorless prism crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05728835 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-286d645aee2846f5b4cfba9c154358d8 |
| Source note | uspto-grants-1998_03 |