Water → HCID 131714190, compound
Reaction equation
Cl[Si:2](Cl)(Cl)[CH2:3][CH2:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][N:6]=1.O>CO>[SiH3:2][CH2:3][CH2:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][N:6]=1Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
A solution of 2-(2-silylethyl)pyridine oligosilsesquioxane pillar material was prepared from a methanol solution of 2-(2-trichlorosilylethyl)pyridine (24 grams of 2-(2-trichlorosilylethyl)pyridine in 175 ml of methanol by adding 10.5 ml of water. The mixture was stirred for 1 hour while maintaining the temperature below 30° C.
Workup
- temperaturewhile maintaining the temperature below 30° C.
Sources & evidence
- ORD record
- ord-b4cfba36d9ea4d0d897c1276927d49db
- Source dataset
- uspto-grants-1988_01
- Patent number
- US04717513
Reaction notes
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