4-Methyl-2-pentylpyridine → HCID 67451102, compound

HRID 241483Notes

Reaction equation

HRID 241483 reaction equation
C[C:2]1[CH:7]=[CH:6]N=[C:4]([CH2:8]CCCC)[CH:3]=1.C([Mg]Br)CCCCC.Cl[C:22]1[CH:27]=[C:26]([CH2:28][CH3:29])[CH:25]=[CH:24][N:23]=1>>[CH2:28]([C:26]1[CH:25]=[CH:24][N:23]=[C:22]([CH2:6][CH2:7][CH2:2][CH2:3][CH2:4][CH3:8])[CH:27]=1)[CH3:29]

Participants

4

Reactant 3

HCID 30200104-Methyl-2-pentylpyridineHCID 36534732-Chloro-4-ethylpyridineHCID 178444609HCID 178444609, compound

Product 1

HCID 67451102HCID 67451102, compound

Procedure

This compound was obtained using the same experimental procedure as per 4-methyl-2-pentyl-pyridine (see above), using hexyl magnesium bromide instead of pentyl magnesium bromide and 2-chloro-4-ethyl pyridine instead of 2-bromo-4-methylpyridine. The product was obtained with similar yield and purified in the same way.

Workup

  1. customThis compound was obtained
  2. customThe product was obtained
  3. customwith similar yield
  4. custompurified in the same way

Sources & evidence

ORD record
ord-1b440411a4b44ef8859a5c6b53b24894
Source dataset
uspto-grants-2014_02
Patent number
US08652452B2

Reaction notes

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