HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nitrobenzoic acid → N-(3-methoxyphenyl)-3-nitrobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nitrobenzoic acid | HCID 8497 | — |
| Reactant | 3-Methoxyaniline | HCID 10824 | — |
| Product | N-(3-methoxyphenyl)-3-nitrobenzamide | HCID 306640 | 91.3% |
Reaction Steps
Using m-anisidine (2.03 g, 16.5 mmol) and 3-nitrobenzoic acid (2.51 g, 15.0 mmol), the procedure of Reference Example 16 was repeated to obtain 3.72 g (91.3%) of the title compound in the form of colorless powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05728835 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-328ffea84e8945bab5f2c5c05d92ed2e |
| Source note | uspto-grants-1998_03 |