HuagongsheHuagongshe Chemistry Print Report · For research reference only
P-Anisidine → 3-Methoxy-4-nitro-N-(4-methoxyphenyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | P-Anisidine | HCID 7732 | — |
| Reactant | 3-Methoxy-4-nitrobenzoic acid | HCID 78764 | — |
| Product | 3-Methoxy-4-nitro-N-(4-methoxyphenyl)benzamide | HCID 19690048 | 92.7% |
Reaction Steps
Using p-anisidine (738 mg, 6.0 mmol) and 3-methoxy-4-nitrobenzoic acid (986 mg, 5.0 mmol), the procedure of Reference Example 16 was repeated to obtain 1.40 g (92.7%) of the title compound in the form of colorless powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05728835 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-d6f0bef2d28347ca947ceb2e3c17a182 |
| Source note | uspto-grants-1998_03 |