HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzoic Acid → N-(4-Methylphenyl)-4-nitrobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzoic Acid | HCID 6108 | — |
| Reactant | p-Toluidine | HCID 7813 | — |
| Product | N-(4-Methylphenyl)-4-nitrobenzamide | HCID 591812 | 99.6% |
Reaction Steps
Using p-toluidine (1.19 g, 11.0 mmol) and 4-nitrobenzoic acid (1.77 g, 10.5 mmol), the procedure of Reference Example 16 was repeated to obtain 2.68 g (99.6%) of the title compound in the form of light yellow needle crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05728835 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-225d5fd599ed478295e732ac8190f2ec |
| Source note | uspto-grants-1998_03 |