HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nitrobenzoic acid → 4'-Fluoro-3-nitrobenzanilide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nitrobenzoic acid | HCID 8497 | — |
| Reactant | 4-Fluoroaniline | HCID 9731 | — |
| Product | 4'-Fluoro-3-nitrobenzanilide | HCID 765293 | 76.1% |
Reaction Steps
Using 4-fluoroaniline (1.1 ml, 10.9 mmol) and 3-nitrobenzoic acid (1.76 g, 10.0 mmol), the procedure of Reference Example 16 was repeated to obtain 1.98 g (76.0%) of the title compound in the form of light yellow needle crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05728835 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-29a2732da3a948f4aae1ec2e95eeccf2 |
| Source note | uspto-grants-1998_03 |