HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nitrobenzoic acid → N-[3-(methylsulfanyl)phenyl]-3-nitrobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nitrobenzoic acid | HCID 8497 | — |
| Reactant | Benzenamine, 3-(methylthio)- | HCID 15693 | — |
| Product | N-[3-(methylsulfanyl)phenyl]-3-nitrobenzamide | HCID 895917 | 94.6% |
Reaction Steps
Using 3-methylthioaniline (2.1 ml, 16.5 mmol) and 3-nitrobenzoic acid (2.64 g, 15.0 mmol), the procedure of Reference Example 16 was repeated to obtain 4.09 g (94.6%) of the title compound in the form of light yellow needle crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05728835 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-c16cf1c3e2df4892b6f3150e9b21bcaf |
| Source note | uspto-grants-1998_03 |