HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzoic Acid → N-(3,5-dimethylphenyl)-4-nitrobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzoic Acid | HCID 6108 | — |
| Reactant | 3,5-Dimethylaniline | HCID 7949 | — |
| Product | N-(3,5-dimethylphenyl)-4-nitrobenzamide | HCID 2843294 | — |
Reaction Steps
Using 3,5-xylidine (1.42 ml, 11.0 mmol) and 4-nitrobenzoic acid (1.76 g, 10.4 mmol), the procedure of Reference Example 16 was repeated to obtain 2.72 g (quantitative) of the title compound in the form of light yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05728835 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-faf03e3b2ef74ea6adbc16e6e6d66bc2 |
| Source note | uspto-grants-1998_03 |