1-Iodohexane → HCID 15030189, compound

HRID 248180

Reaction equation

I[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH3:7].[OH:8][C:9]1[CH:10]=[C:11]2[C:16](=[CH:17][CH:18]=1)[CH:15]=[C:14]([CH:19]([CH3:23])[C:20]([OH:22])=[O:21])[CH:13]=[CH:12]2>>[CH3:23][CH:19]([C:14]1[CH:13]=[CH:12][C:11]2[C:16](=[CH:17][CH:18]=[C:9]([O:8][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH3:7])[CH:10]=2)[CH:15]=1)[C:20]([OH:22])=[O:21]

Participants

Reactant 2

HCID 125271-Iodohexane

HCID 162920Desmethylnaproxen

Product 1

HCID 15030189HCID 15030189, compound

Procedure

The title compound is prepared according to the method of Example 7 using 1-iodohexane and racemic 6-hydroxy-α-methyl-2-naphthaleneacetic acid. White crystals are obtained having a melting point of 88°-91° C.

Workup

customWhite crystals are obtained

Sources & evidence

ORD record: ord-62f24be2a6f448e79f7642fd2c7b6fdb
Source dataset: uspto-grants-1993_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05208344

Linked notes

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