Acetate → Aluminum Acetate

HRID 252437

Reaction equation

HRID 252437 reaction equation
[Cl-].[Al+3:2].[Cl-].[Cl-].[C:5]([O-:8])(=[O:7])[CH3:6]>O>[C:5]([O-:8])(=[O:7])[CH3:6].[Al+3:2].[C:5]([O-:8])(=[O:7])[CH3:6].[C:5]([O-:8])(=[O:7])[CH3:6]

Participants

4

Reactant 2

HCID 175AcetateHCID 6451240Aluminum(III) Chloride

Product 1

HCID 8757Aluminum Acetate

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Aqueous basic aluminum chloride solution of concentration of 5.0% by weight on the basis of Al2O3 was produced by diluting commercialized aqueous basic aluminum chloride solution (23.5% by weight on the basis of Al2O3, 8.15% by weight of chloride ion, 83.3% of basicity, and pH 4.0) with pure water. The aqueous solution was passed through an acetate-type anion exchange resin column at space velocity 5 to obtain an aqueous basic aluminum acetate solution. The obtained aqueous solution was dried at 90° C. and atmospheric pressure to adjust the water content to be 20% to obtain a basic aluminum acetate solid. The obtained solid had 0.79 in a full width at half maximum of the peak measured by the x-ray diffractiometry described in the above-mentioned evaluation method.

Workup

  1. additionby diluting

Sources & evidence

ORD record
ord-ec8c49b5b9d944bc9efc1dbd783b8dd4
Source dataset
uspto-grants-2011_01
Patent number
US07868126B2

Linked notes

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