HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Alcohol → Benzyl fluoroformate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | Sodium Fluoride | HCID 5235 | — |
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | Benzyl fluoroformate | HCID 3023023 | — |
Reaction Steps
The process is performed as in Example 1 with, in the first reactor, 168 g (4 mol) of sodium fluoride powder having the same characteristics as described in Example 1 and 320 ml of acetonitrile and, in the second reactor, 108 g (1 mol) of benzyl alcohol, 50.5 g (1.2 mol) of sodium fluoride of the same characteristics as above and 150 g of dimethoxyethane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06858751B1 |
| Source dataset | uspto-grants-2005_02 |
| ORD ID | ord-868776c4aa2e4da9aec0e9e64cce3e8d |
| Source note | uspto-grants-2005_02 |