Isopropylamine → HCID 178457516, compound
Reaction equation
C(N[CH:4]=[N:5][C:6]1[CH:11]=[CH:10][C:9]([C:12]2[N:16]=[CH:15][NH:14][N:13]=2)=[CH:8][CH:7]=1)#N.[CH:17]([NH2:20])([CH3:19])[CH3:18]>O>[CH:17]([NH:20][CH:4]=[N:5][C:6]1[CH:11]=[CH:10][C:9]([C:12]2[N:16]=[CH:15][NH:14][N:13]=2)=[CH:8][CH:7]=1)([CH3:19])[CH3:18]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
A solution of N-Cyano-N'-[4-(1,2,4-triazol-3-yl)-phenyl]-formamidine (3 g) and isopropylamine (8.5 g) in water (1.5 ml) was stirred for twenty minutes. The crystallized solid was filtered off and purified via its maleate salt in ethanol.
Workup
- filtrationThe crystallized solid was filtered off
- custompurified via its maleate salt in ethanol
Sources & evidence
- ORD record
- ord-fe2fe274ad4e4573b6aea4ebe09a8706
- Source dataset
- uspto-grants-1987_10
- Patent number
- US04699915
Reaction notes
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