HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Malonate → Diethyl 2-[(1-tridecynyl)phenyl]methylenepropan-1,3-dioate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Malonate | HCID 7761 | — |
| Reactant | 2-(1-Tridecynyl)benzaldehyde | HCID 13688501 | — |
| Product | Diethyl 2-[(1-tridecynyl)phenyl]methylenepropan-1,3-dioate | HCID 20165387 | — |
Reaction Steps
A solution of 2-(1-tridecynyl)benzaldehyde (6.42, 22.6 mmol from example 3) was condensed with diethyl malonate (3.72 g) as described in example 1 to give 2.00 g (21%, 36% on the basis of unrecovered starting material) of the title compound identical with that prepared in example 6 above.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04699995 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-62f05dd6140a4f23af3c4f8e6bc03328 |
| Source note | uspto-grants-1987_10 |