HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Buten-1-amine → HCID 178457207, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Buten-1-amine | HCID 443732 | — |
| Reactant | 3,4-Difluorophenyl chloroformate | HCID 22567999 | — |
| Reactant | HCID 178484797 | HCID 178484797 | — |
| Product | HCID 178457207 | HCID 178457207 | — |
Reaction Steps
In analogy to examples 29.10 and 29.11, trans-Methansulfonic acid 5-(4-methyl amino-cyclohexyl)-pentyl ester-Trifluoroacetic acid salt and 3,4-difluoro-phenyl chloroformate were reacted, followed by treatment with N-allylmethylamine to yield trans-{4-[5-(Allyl-methyl-amino)-pentyl]-cyclohexyl}-methyl-carbamic acid 3,4-difluoro-phenyl ester, MS: 409 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06858651B2 |
| Source dataset | uspto-grants-2005_02 |
| ORD ID | ord-27efb7bec3cd4780bf83f5e4a963c53c |
| Source note | uspto-grants-2005_02 |