HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylenetetramine → Ethylene carbonate triethylene tetraamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylenetetramine | HCID 5565 | — |
| Reactant | Ethylene carbonate | HCID 7303 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Ethylene carbonate triethylene tetraamine | HCID 86740738 | — |
Reaction Steps
Add 2 g of triethylene tetraamine (with an AV of approximately 1180 mg KOH/g) to 20 ml of toluene in a 250 ml flask fitted with a stirrer, condensor and nitrogen inlet. Add 1.21 g ethylene carbonate to the mixture. Reflux the system for 2.5 hours under N2. Strip the system to yield an ethylene carbonate-triethylene tetraamine adduct having an AV of approximately 507 mg KOH/g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04702851 |
| Source dataset | uspto-grants-1987_10 |
| ORD ID | ord-f616fe48cf504a7ca3dc8d61d722a7fa |
| Source note | uspto-grants-1987_10 |