HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Iodoaniline → N-(4-iodophenyl)-N-methylethanesulphonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Iodoaniline | HCID 10893 | — |
| Reactant | Ethanesulfonyl chloride | HCID 11667 | — |
| Reactant | N-(4-iodophenyl)methanesulfonamide | HCID 836147 | — |
| Product | N-(4-iodophenyl)-N-methylethanesulphonamide | HCID 19785600 | — |
Reaction Steps
The product so obtained was used in place of 4-iodoaniline in the procedure described in Example 3 for the preparation of N-(4-iodophenyl) methanesulphonamide and ethanesulphonyl chloride was used in place of methanesulphonyl chloride. Thus was obtained N-(4-iodophenyl)-N-methylethanesulphonamide as an oil. NMR Spectrum 1.45 (3H, t), 3.00 (2H, q), 3.35 (3H, s), 7.15 (2H, m), 7.70 (2H, m).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05258399 |
| Source dataset | uspto-grants-1993_11 |
| ORD ID | ord-5611fef512954a2ea8368584f719a99e |
| Source note | uspto-grants-1993_11 |