alpha-Hydroxyacetophenone → 4-Vinylbenzaldehyde

HRID 256702

Reaction equation

[CH:1]([C:3]1[CH:20]=[CH:19][C:6]([C:7]2[O:8]C3C(C(=O)C=2O)=CC=CC=3)=[CH:5][CH:4]=1)=[CH2:2].OCC(C1C=CC=CC=1)=O>>[CH:1]([C:3]1[CH:20]=[CH:19][C:6]([CH:7]=[O:8])=[CH:5][CH:4]=1)=[CH2:2]

Participants

Reactant 2

HCID 68490alpha-Hydroxyacetophenone

HCID 109014724'-Vinyl-3-hydroxyflavone

Product 1

HCID 393894-Vinylbenzaldehyde

Procedure

4'-vinyl-3-hydroxyflavone. 2-hydroxyacetophenone (Aldrich) was used as received. Ethyl alcohol was distilled prior to use. 4-vinyl benzaldehyde was synthesized using the procedure described in Example 1(a).

Workup

distillationEthyl alcohol was distilled

Sources & evidence

ORD record: ord-e1d086e52ada4775a962c4774dfca4d4
Source dataset: uspto-grants-1993_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05258478

Linked notes

Loading…