Phenyl isocyanate → Acetanilide

HRID 257239

Reaction equation

HRID 257239 reaction equation
[C:1]1([N:7]=[C:8]=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[N-:10]=[C:11]=O>C(O)(=O)C>[C:1]1([NH:7][C:8](=[O:9])[NH:10][C:11]2[CH:5]=[CH:6][CH:1]=[CH:2][CH:3]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[C:8]([NH:7][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)(=[O:9])[CH3:11]

Participants

5

Reactant 2

HCID 7672Phenyl isocyanateHCID 105034Isocyanate

Product 2

HCID 904AcetanilideHCID 7595Carbanilide

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent2×

Procedure

1.19 g phenyl isocyanate and 0.6 g acetic acid were reacted in a 1:1 isocyanate:acetic acid molar ratio. The reaction, product isolation and analysis were conducted as in Example 1. 0.45 g diphenyl urea and 0.9 g acetanilide were obtained.

Workup

  1. customThe reaction, product isolation and analysis

Sources & evidence

ORD record
ord-c3d0a39d32c549c79511e491efbc746a
Source dataset
uspto-grants-1993_11
Patent number
US05260483

Linked notes

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