Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | Isodecanol | HCID 32898 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | Isodecyl acrylate | HCID 14899 | — |
Reaction Steps
To 157 g isodecyl alcohol in 200 ml xylene is added 117 g AA, 1.0 g HQ and 2.0Q PTSA. The reaction mixture is heated for 2 hrs. at reflux (140° C) while the water of reaction is collected (17 ml). The reaction mixture is cooled and the xylene removed under reduced pressure to give 250 g isodecyl acrylate. The analytical data for this acrylate is shown below.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04035409 |
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| Source dataset | uspto-grants-1977_07 |
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| ORD ID | ord-7aeb45784b7e46019546e24d9d59e0ae |
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| Source note | uspto-grants-1977_07 |
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