Phenoxyethanol → 2-Phenoxyethyl (chloroacetyl)carbamate

HRID 259299

Reaction equation

HRID 259299 reaction equation

[Cl:1][CH2:2][C:3]([N:5]=[C:6]=[O:7])=[O:4].[O:8]([CH2:15][CH2:16][OH:17])[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1>C1C=CC=CC=1>[Cl:1][CH2:2][C:3]([NH:5][C:6](=[O:7])[O:17][CH2:16][CH2:15][O:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)=[O:4]

Participants

4

Reactant 2

HCID 31236Phenoxyethanol

HCID 78209Chloroacetyl isocyanate

Product 1

HCID 214241892-Phenoxyethyl (chloroacetyl)carbamate

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

Chloroacetylisocyanate (12g) was added slowly to the solution of β-phenoxyethylalcohol (13.8g) and benzene (100ml) at room temperature.

Sources & evidence

ORD record: ord-e83dbd801bde4358b673de12d40787d2
Source dataset: uspto-grants-1977_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04036984

Linked notes

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