HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphinic Acid → 1-Benzhydrylamino-2-methylpropanephosphonous acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphinic Acid | HCID 4124402 | — |
| Reactant | Isobutylidenebenzhydrylamine | HCID 10657527 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-Benzhydrylamino-2-methylpropanephosphonous acid | HCID 21325882 | — |
Reaction Steps
Hypophosphorous acid (100%, 15.8 parts) dissolved in absolute ethanol was added to a stirred solution of 41.3 parts isobutylidenebenzhydrylamine in absolute ethanol. An exothermic reaction occurred. After standing one hour the reaction was filtered and the white solid dried in vacuo. There was obtained DL-1-benzhydrylamino-2-methylpropanephosphonous acid, melting point 191° (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04147780 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-bee6e3df24624b6d98464e0a489e9362 |
| Source note | uspto-grants-1979_04 |