Sodium Carbonate → alpha-(5-Indenoxy)acetophenone

HRID 262535

Reaction equation

HRID 262535 reaction equation
[OH:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][CH:10]=1)[CH2:7][CH2:6][CH2:5]2.Cl[CH2:12][C:13]([C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)=[O:14].C(=O)([O-])[O-].[Na+].[Na+]>C1C=CC=CC=1>[CH2:7]1[C:8]2[C:4](=[CH:3][C:2]([O:1][CH2:12][C:13]([C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=3)=[O:14])=[CH:10][CH:9]=2)[CH:5]=[CH:6]1

Participants

5

Reactant 3

HCID 10340Sodium CarbonateHCID 107572-ChloroacetophenoneHCID 151185-Indanol

Product 1

HCID 20563333alpha-(5-Indenoxy)acetophenone

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

Using the method of Example 1, step A, 5-hydroxyindane is reacted with α-chloroacetophenone in benzene in the presence of sodium carbonate to provide α-(5-indenoxy) acetophenone as a yellow solid.

Sources & evidence

ORD record
ord-0cab73b087444407a4525dab45f83d00
Source dataset
uspto-grants-1979_05
Patent number
US04154848

Linked notes

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