HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 263139Generated: October 26, 2026
Water → 2-Cyclohexenyl 2-cyclopentenyl ether
https://huagongshe.com/reaction/263139
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 2-Cyclohexen-1-OL | HCID 13198 | — |
| Reactant | Acetic acid, cyclopent-2-en-1-yl ester | HCID 140735 | — |
| Catalyst | Tetrabutylammonium hydrogen sulfate | HCID 94433 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 2-Cyclohexenyl 2-cyclopentenyl ether | HCID 21318237 | — |
Reaction Steps
A two-phase reaction mixture containing 2-cyclopentenyl acetate (0.30 g, 2.4 millimols), 2-cyclohexenol (0.50 g, 5.1 millimols), tetrabutylammonium hydrogen sulfate (0.020 g, 0.06 millimols), and water (0.25 g, 13.9 millimols) was heated at 40° C. with vigorous stirring for four hours. Acetone was then added to give a one-phase system for analytical purposes, and the solution was analyzed by gas chromatography using an Apiezon column programmed from 60° to 220° C. The following relative peak areas were observed for the cyclic components:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04156097 |
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| Source dataset | uspto-grants-1979_05 |
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| ORD ID | ord-6bc7b792bc83400f91e2a4e27b1d9525 |
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| Source note | uspto-grants-1979_05 |
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