HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methylbenzo[b]thiophene → 2-(4-Chloro-3-sulfamoylbenzoyl)-3-methyl-benzo[b]thiophene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methylbenzo[b]thiophene | HCID 73817 | — |
| Reactant | 3-(Aminosulfonyl)-4-chlorobenzoyl chloride | HCID 3017979 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Chlorobenzene | HCID 7964 | — |
| Product | 2-(4-Chloro-3-sulfamoylbenzoyl)-3-methyl-benzo[b]thiophene | HCID 21316639 | — |
Reaction Steps
is obtained as described in Example 1 from 2.5 g 4-chloro-3-sulfamoylbenzoyl chloride, 1.6 g 3-methylbenzo[b]thiophene and 3 g aluminum chloride in 50 ml chlorobenzene. Colorless crystals, m.p. 210° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04156732 |
| Source dataset | uspto-grants-1979_05 |
| ORD ID | ord-c924855fb6344a32ab7dcacaf651a47f |
| Source note | uspto-grants-1979_05 |