HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 2-(1H-Imidazol-1-yl)-1-(2-naphthalenyl)ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Nafimidone monohydrochloride | HCID 51199 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2-(1H-Imidazol-1-yl)-1-(2-naphthalenyl)ethanone | HCID 51200 | — |
Reaction Steps
1-(2-Naphthoylmethyl)imidazole hydrochloride (1.0 g.) suspended in 50 ml. of ether is stirred with excess dilute aqueous potassium carbonate solution until the salt is completely dissolved. The organic layer is then separated, washed twice with water, dried over magnesium sulfate and evaporated to yield 1-(2-naphthoylmethyl)imidazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04150153 |
| Source dataset | uspto-grants-1979_04 |
| ORD ID | ord-db5c8d01e01c4b6882b725e1358bba66 |
| Source note | uspto-grants-1979_04 |