4-(3-Methylbutyl)-4-phenyl-4-silacyclohexanone → HCID 178418246, compound

HRID 2657

Reaction equation

HRID 2657 reaction equation
[CH3:1][CH:2]([CH3:18])[CH2:3][CH2:4][Si:5]1(C2C=CC=CC=2)[CH2:10][CH2:9][C:8](=O)[CH2:7][CH2:6]1.Br[C:20]1[CH:25]=[CH:24][C:23]([C:26]([F:29])=[CH:27][F:28])=[CH:22][CH:21]=1>>[CH3:18][CH:2]([CH3:1])[CH2:3][CH2:4][Si@H:5]1[CH2:6][CH2:7][C@H:8]([C:20]2[CH:25]=[CH:24][C:23]([C:20]3[CH:25]=[CH:24][C:23]([C:26]([F:29])=[CH:27][F:28])=[CH:22][CH:21]=3)=[CH:22][CH:21]=2)[CH2:9][CH2:10]1

Participants

3

Reactant 2

HCID 195938624-(3-Methylbutyl)-4-phenyl-4-silacyclohexanoneHCID 539837551-Bromo-4-(1,2-difluoroethenyl)benzene

Product 1

HCID 178418246HCID 178418246, compound

Procedure

The general procedure of Example 35 was repeated using 4-(3-methylbutyl)-4-phenyl-4-silacyclohexanone instead of 4-pentyl-4-phenyl-4-silacyclohexanone and 4-bromo-1-(1,2-difluorovinyl)benzene instead of 4-bromo-2,6-difluoro-1-(2,2-difluorovinyloxy)benzene, thereby obtaining the intended compound.

Workup

  1. customobtaining the intended compound

Sources & evidence

ORD record
ord-af2f9c6c94004dd4808d0d3c80050cd2
Source dataset
uspto-grants-1998_03
Patent number
US05730901

Linked notes

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