Dicyclohexylcarbodiimide → 2-Dimethylaminopyridine

HRID 266176

Reaction equation

HRID 266176 reaction equation
[CH3:1][C@H]1OC(=O)C2C(O)=CC(O)=C(Cl)C=2CC(=O)C=CC=C[C@H]2O[C@H]2C1.C(O)(=O)CCCCCCC/C=C\CCCCCC.[CH:44]1([N:50]=[C:51]=[N:52][CH:53]2[CH2:58][CH2:57][CH2:56]CC2)CCCCC1>C(Cl)Cl>[CH3:1][N:50]([C:51]1[CH:56]=[CH:57][CH:58]=[CH:53][N:52]=1)[CH3:44]

Participants

5

Reactant 3

HCID 10868DicyclohexylcarbodiimideHCID 445638Palmitoleic AcidHCID 11268547CID 11268547

Product 1

HCID 218852-Dimethylaminopyridine

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

Following a procedure similar to that described in Example 12, but using 365 mg of radicicol, 636 mg of palmitoleic acid, 20 ml of dry methylene chloride, 716 mg of dicyclohexylcarbodiimide and a catalytic amount of dimethylaminopyridine, 654 mg of the title compound were obtained.

Sources & evidence

ORD record
ord-7627f8efa55d47fa8859bfb560c11ae1
Source dataset
uspto-grants-1997_07
Patent number
US05650430

Linked notes

Loading…