2-Bromophenol → o-Bromo-phenyl 1,5-dimethyl-hexyl ether

HRID 267708

Reaction equation

Br[CH:2]([CH2:4][CH2:5][CH2:6][CH:7]([CH3:9])[CH3:8])[CH3:3].[Br:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][C:12]=1[OH:17]>>[CH3:3][CH:2]([O:17][C:12]1[CH:13]=[CH:14][CH:15]=[CH:16][C:11]=1[Br:10])[CH2:4][CH2:5][CH2:6][CH:7]([CH3:9])[CH3:8]

Participants

Reactant 2

HCID 72442-Bromophenol

HCID 1383322-Bromo-6-methylheptane

Product 1

HCID 21487568o-Bromo-phenyl 1,5-dimethyl-hexyl ether

Procedure

In the same manner as Example 1: 2-bromo- 6-methyl-heptane was reacted with o-bromo-phenol to obtain o-bromo-phenyl 1,5-dimethyl-hexyl ether (boiling point = 190°-193°C/17 mmHg);

Sources & evidence

ORD record: ord-08b5d6f2636547978a9c5cc37ada80ed
Source dataset: uspto-grants-1976_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03944531

Linked notes

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