Diisobutylamine → p-[(1,5-dimethyl-hexyl)-oxy]-N,N-diisobutylbenzamide

Reaction equation

[CH2:1]([NH:5][CH2:6][CH:7]([CH3:9])[CH3:8])[CH:2]([CH3:4])[CH3:3].CO[C:12](=[O:28])[C:13]1[CH:18]=[CH:17][C:16]([O:19][CH:20]([CH3:27])[CH2:21][CH2:22][CH2:23][CH:24]([CH3:26])[CH3:25])=[CH:15][CH:14]=1>>[CH3:27][CH:20]([O:19][C:16]1[CH:15]=[CH:14][C:13]([C:12]([N:5]([CH2:6][CH:7]([CH3:9])[CH3:8])[CH2:1][CH:2]([CH3:4])[CH3:3])=[O:28])=[CH:18][CH:17]=1)[CH2:21][CH2:22][CH2:23][CH:24]([CH3:25])[CH3:26]

Participants

Reactant 2

HCID 8085Diisobutylamine

HCID 54404637HCID 54404637, compound

Product 1

HCID 21487604p-[(1,5-dimethyl-hexyl)-oxy]-N,N-diisobutylbenzamide

Procedure

By the procedure given in Example 37, diisobutylamine is reacted with p-[(1,5-dimethyl-hexyl)-oxy]-benzoic acid methyl ester to produce p-[(1,5-dimethyl-hexyl)-oxy]-N,N-diisobutyl-benzamide (nD24 = 1.4968).

Sources & evidence

ORD record: ord-19f982faf5d441b5b524ccb9e2899ff6
Source dataset: uspto-grants-1976_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03944531

Reaction notes

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