HCID 178479391, compound → HCID 178512583, compound

HRID 27192

Reaction equation

HRID 27192 reaction equation
Cl.[Cl:2][C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([Cl:9])[C:4]=1[NH:10][C:11]([NH2:13])=[NH:12]>[OH-].[Na+]>[Cl:2][C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([Cl:9])[C:4]=1[NH:10][C:11]([NH2:13])=[NH:12]

Participants

3

Reactant 1

HCID 178479391HCID 178479391, compound

Product 1

HCID 178512583HCID 178512583, compound

Reagents, catalysts & solvents 1

HCID 14798Sodium HydroxideSolvent

Procedure

The free base is prepared by dissolving 2,6-dichlorophenylguanidine hydrochloride in 10% sodium hydroxide solution and extracting with ether. The ether is dried and evaporated to dryness to obtain 2,6-dichlorophenylguanidine.

Workup

  1. customThe free base is prepared
  2. extractionextracting with ether
  3. dry with materialThe ether is dried
  4. customevaporated to dryness

Sources & evidence

ORD record
ord-a44b08c76d374b0796f109e5b67e825d
Source dataset
uspto-grants-1980_09
Patent number
US04220658

Linked notes

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