Ethyl isobutyrate → Ethyl 6-bromo-2,2-dimethylhexanoate

HRID 274290Notes

Reaction equation

[C:1]([O:6][CH2:7][CH3:8])(=[O:5])[CH:2]([CH3:4])[CH3:3].[Br:9][CH2:10][CH2:11][CH2:12][CH2:13]Br>>[Br:9][CH2:10][CH2:11][CH2:12][CH2:13][C:2]([CH3:4])([CH3:3])[C:1]([O:6][CH2:7][CH3:8])=[O:5]

Participants

Reactant 2

HCID 7342Ethyl isobutyrate

HCID 80561,4-Dibromobutane

Product 1

HCID 10444833Ethyl 6-bromo-2,2-dimethylhexanoate

Procedure

Using ethyl isobutyrate and 1,4-dibromobutane, the same reaction as in Reference Example 16 was conducted to produce the title compound. b.p. 62°-64° C./0.4 mmHg

Workup

customthe same reaction as in Reference Example 16

Sources & evidence

ORD record: ord-361c836d642547cb80dc49089ba624f5
Source dataset: uspto-grants-1995_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05389633

Reaction notes

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