1,4-Dibromobutane → Ethyl 6-bromo-2,2-diethylhexanate

Reaction equation

[CH2:1]([CH:3]([CH2:9][CH3:10])[C:4]([O:6][CH2:7][CH3:8])=[O:5])[CH3:2].[Br:11][CH2:12][CH2:13][CH2:14][CH2:15]Br>>[Br:11][CH2:12][CH2:13][CH2:14][CH2:15][C:3]([CH2:9][CH3:10])([CH2:1][CH3:2])[C:4]([O:6][CH2:7][CH3:8])=[O:5]

Participants

Reactant 2

HCID 80561,4-Dibromobutane

HCID 76326Ethyl 2-ethylbutyrate

Product 1

HCID 10516776Ethyl 6-bromo-2,2-diethylhexanate

Procedure

Using ethyl 2-ethylbutyrate and 1,4-dibromobutane, the same reaction as in Reference Example 16 was conducted to produce the title compound. b.p. 125°-130° C./0.3 mmHg

Workup

customthe same reaction as in Reference Example 16

Sources & evidence

ORD record: ord-33350e08be0048d09bf54717a42189b2
Source dataset: uspto-grants-1995_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05389633

Reaction notes

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