2-Chloroethylammonium chloride → HCID 178428748, compound

HRID 276430

Reaction equation

HRID 276430 reaction equation
[Cl-].Cl[CH2:3][CH2:4][NH3+:5].[CH3:6][C:7]1[CH:12]=[C:11]([N+:13]([O-:15])=[O:14])[CH:10]=[CH:9][C:8]=1[N:16]=[C:17]=[S:18]>>[CH3:6][C:7]1[CH:12]=[C:11]([N+:13]([O-:15])=[O:14])[CH:10]=[CH:9][C:8]=1[N:16]=[C:17]1[NH:5][CH2:4][CH2:3][S:18]1

Participants

3

Reactant 2

HCID 133682-Chloroethylammonium chlorideHCID 1456212-Methyl-4-nitrophenyl isothiocyanate

Product 1

HCID 178428748HCID 178428748, compound

Procedure

2-Chloroethylammonium chloride (Entry 1) was reacted with 2-methyl-4-nitrophenyl isothiocyanate according to Method C1a to give 2-(2-methyl-4-nitrophenylimino)-1,3-thiazolidine, which was reacted with 5-(bromomethyl)bicyclo[2.2.1]hept-2-ene according to Method D2a to give 2-(4-nitrophenylimino)-3-((bicyclo[2.2.1]hept-2-en-5-yl)methyl)-1,3 -thiazolidine.

Sources & evidence

ORD record
ord-511e3ae49e0e4a6aba480d9f436aba29
Source dataset
uspto-grants-2002_03
Patent number
US06353006B1

Linked notes

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