HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → N-(3-benzoylphenyl)-4-chlorobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| Reactant | Methanone, (3-aminophenyl)phenyl- | HCID 17817 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | N-(3-benzoylphenyl)-4-chlorobenzamide | HCID 721817 | — |
Reaction Steps
With agitation, 4.9 g 4-chlorobenzoyl chloride are added bit by bit to a solution, cooled to 5° C., of 5 g 3-amino-benzophenone in 60 ml dimethylacetamide, in the presence of 4.9 g triethylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04223039 |
| Source dataset | uspto-grants-1980_09 |
| ORD ID | ord-a9355115fe224833bb176592d5ae49f2 |
| Source note | uspto-grants-1980_09 |