HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Ethylbenzoic Acid → 4-Ethylbenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Ethylbenzoic Acid | HCID 12086 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | 4-Ethylbenzoyl chloride | HCID 85368 | — |
Reaction Steps
200 g (1.33 millimoles) of 4-ethylbenzoic acid are added rapidly to 500 ml of thionyl chloride with stirring. The mixture is heated at the reflux temperature for 4 hours. After evaporation of the SOCl2 and distillation, 4-ethylbenzoyl chloride is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04588748 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-26a1f02e2dba46d39f0ba1c267c7aba8 |
| Source note | uspto-grants-1986_05 |