Ethanol → HCID 23320751, compound
Reaction equation
[CH2:1]([OH:3])[CH3:2].Cl[C:5]1[C:9]2[C:10]([N+:14]([O-:16])=[O:15])=[CH:11][CH:12]=[CH:13][C:8]=2[S:7](=[O:18])(=[O:17])[N:6]=1>ClCCl>[CH2:1]([O:3][C:5]1[C:9]2[C:10]([N+:14]([O-:16])=[O:15])=[CH:11][CH:12]=[CH:13][C:8]=2[S:7](=[O:17])(=[O:18])[N:6]=1)[CH3:2]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
Ethanol (100 ml) was added to a solution of 3-chloro-4-nitro-benzoisothiazole-1,1-dioxide (0.86 g) in dichloromethane (110 ml). The resulting solution was allowed to stand overnight at room temperature. Removal of the solvent in vacuo gave an amorphous brown solid, which was triturated under ether (100 ml) to give the title compound as a white solid (0.82 g), mpt 190°-191° C.
Workup
- customRemoval of the solvent in vacuo
- customgave an amorphous brown solid, which
- customwas triturated under ether (100 ml)
Sources & evidence
- ORD record
- ord-1d7fbeee813a499892bfbfd33c9e0697
- Source dataset
- uspto-grants-1986_05
- Patent number
- US04590192
Reaction notes
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