HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Anilinopropionitrile → 3-Anilino-2-(3-benzo[b]thienylmethyl)acrylonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Anilinopropionitrile | HCID 14100 | — |
| Reactant | 1-Benzothiophene-3-carbaldehyde | HCID 227328 | — |
| Solvent | Water | HCID 962 | — |
| Product | 3-Anilino-2-(3-benzo[b]thienylmethyl)acrylonitrile | HCID 70474354 | — |
Reaction Steps
The title compound was prepared from thianaphthene-3-carboxaldehyde (W. J. King and F. F. Nord, J. Org. Chem. 1948, 13, 635) and 3-anilinopropionitrile by the procedure of Example 4A (29%); mp 168°-170° dec. Anal. Calcd for C18H14N2S: 0.1 H2O: C, 73.99; H, 4.90; N, 9.59; S, 10.97. Found: C, 74.03; H, 5.21; N, 9.59; S, 11.01.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04590271 |
| Source dataset | uspto-grants-1986_05 |
| ORD ID | ord-55d7daeaea624124a8432373072b9aee |
| Source note | uspto-grants-1986_05 |