HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylthiazole → 2-(4-Methyl-2-thiazolyl)-2-(2-thienyl)tetrahydrofuran
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylthiazole | HCID 12748 | — |
| Reactant | 4-Chloro-1-(2-thienyl)butan-1-one | HCID 123511 | — |
| Product | 2-(4-Methyl-2-thiazolyl)-2-(2-thienyl)tetrahydrofuran | HCID 18936303 | — |
Reaction Steps
The title compound was prepared from 4-methylthiazole and 4-chloro-1-(2-thienyl)-1-butanone, using the general method of Example 36. M.p. 59°-60° C., 13C Nmr (CDCl3) 17.4, 26.2, 41.2, 69.3, 86.2, 113.9, 124.2, 124.7, 126.8, 148.9, 153.1 and 175.6 ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05731335 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-47117198c8d046e0b5bd18f8ec9abb21 |
| Source note | uspto-grants-1998_03 |