HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 1-Azido-1-(3-furyl)-1-(4-methyl-5-oxazolyl)ethane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Boron trifluoride | HCID 6356 | — |
| Reactant | Azidotrimethylsilane | HCID 78378 | — |
| Reactant | 1-(3-Furyl)-1-(4-methyl-5-oxazolyl)ethanol | HCID 9794153 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 1-Azido-1-(3-furyl)-1-(4-methyl-5-oxazolyl)ethane | HCID 18936294 | — |
Reaction Steps
1-(3-Furyl)-1-(4-methyl-5-oxazolyl)ethanol (1 g) was suspended in benzene (4 ml). Trimethylsilylazide (822 μl) was added followed by boron trifluoride diethyletherate (770 μl). The mixture was stirred overnight at room temperature, then poured into water and extracted to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05731335 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-d5df902db51f4973b3595b8e30064e32 |
| Source note | uspto-grants-1998_03 |