Reaction equation
[N:1]([C:4]([C:12]1[CH:16]=[CH:15][O:14][CH:13]=1)([C:6]1[O:10][CH:9]=[N:8][C:7]=1[CH3:11])[CH3:5])=[N+]=[N-]>C(O)C.[Pd]>[O:14]1[CH:15]=[CH:16][C:12]([C:4]([NH2:1])([C:6]2[O:10][CH:9]=[N:8][C:7]=2[CH3:11])[CH3:5])=[CH:13]1Participants
4
Reactant 1
Product 1
Reagents, catalysts & solvents 2
Procedure
The product from Example 65 in ethanol was hydrogenated in the presence of 10% palladium-on-charcoal to give the title compound.
Sources & evidence
- ORD record
- ord-dab48b2bfda241a4b7f0f62acf90e643
- Source dataset
- uspto-grants-1998_03
- Patent number
- US05731335
Linked notes
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