HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → Acetoacetamide, N,N-diethyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | Ethyl Acetoacetate | HCID 8868 | — |
| Product | Acetoacetamide, N,N-diethyl- | HCID 16699 | 65.7% |
Reaction Steps
40 g (0.31 mol) of ethyl acetoacetate and 24 g (0.33 mol) of diethylamine were stirred in a Parr apparatus at 150° C. for 10'. The crude mixture was distilled at 115°-120° C./9 mmHg, to give 32 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05731322 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-51c44092234a4bbebe6940b7ac132c46 |
| Source note | uspto-grants-1998_03 |