HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetoacetate → 3-Oxo-n,n-dipropylbutanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetoacetate | HCID 8868 | — |
| Reactant | Dipropylamine | HCID 8902 | — |
| Product | 3-Oxo-n,n-dipropylbutanamide | HCID 249207 | 0.6% |
Reaction Steps
43.4 g (43.3 mol) of ethyl acetoacetate and 33.7 g (43.3 mol) of dipropylamine were treated as described in preparation 1. The crude oil was distilled at 86°-89° C./ 0.8 mmHg, to give 44.3 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05731322 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-9d861ba9b54b4ef8a7a1d9b237766965 |
| Source note | uspto-grants-1998_03 |