HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetoacetanilide → HCID 178418293, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetoacetanilide | HCID 7592 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Benzenediazonium chloride | HCID 60992 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178418293 | HCID 178418293 | 47.6% |
Reaction Steps
4.5 g (25.4 mmol) of acetoacetanilide, a solution of 3.46 g (89 mmol) of NaOH in 45 ml of water and 95 mmol of phenyldiazonium chloride were treated as described in preparation 8. The residue was crystallised from EtOH, yielding 3.4 g of the title compound. M.p.=96°-97° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05731322 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-f388a24479e44c98bc290884466e1ad3 |
| Source note | uspto-grants-1998_03 |