HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2966Generated: October 26, 2026
1,3-Dibromopropane → Dimethyl N-(3-Bromopropyl)iminodiacetate
https://huagongshe.com/reaction/2966
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1,3-Dibromopropane | HCID 8001 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | Dimethyl Iminodiacetate Hydrochloride | HCID 2727727 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Dimethyl N-(3-Bromopropyl)iminodiacetate | HCID 19688438 | — |
Reaction Steps
A mixture of 1 mmol iminodiacetic acid dimethylester hydrochloride salt, 5 mmol N,N-diisopropyl-ethylamine and 3 mmol 1,3-dibromopropane in 2 mL toluene was stirred at 90° C. for 16 h and then chromatographed to provide the title compound as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05731432 |
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| Source dataset | uspto-grants-1998_03 |
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| ORD ID | ord-53859d19f5084c73a9229630dac0c84d |
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| Source note | uspto-grants-1998_03 |
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