HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → Ethyl 3-bromo-4-(bromomethyl)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | Ethyl 3-bromo-4-methylbenzoate | HCID 14945865 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | Ethyl 3-bromo-4-(bromomethyl)benzoate | HCID 13877460 | — |
Reaction Steps
A mixture of 1.0 mmol of ethyl 3-bromo-4-methylbenzoate, 1.0 mmol NBS, and 0.02 mmol benzoyl peroxide in 5 mL CCl4 was refluxed for 4 h and then processed by filtration and chromatography to provide ethyl 3-bromo-4-bromomethylbenzoate as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05731432 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-43fc139c41d84237a967f7fa62214d1c |
| Source note | uspto-grants-1998_03 |