HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2971Generated: October 25, 2026
Tributylvinyltin → Ethyl 2-(3-vinylphenyl)acetate
https://huagongshe.com/reaction/2971
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Tributylvinyltin | HCID 81998 | — |
| Reactant | Ethyl 3-(bromophenyl)acetate | HCID 11470552 | — |
| Catalyst | HCID 178418397 | HCID 178418397 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Ethyl 2-(3-vinylphenyl)acetate | HCID 11687033 | — |
Reaction Steps
A mixture of 1.0 mmol of ethyl 3-bromophenylacetate, 1.5 mmol of vinyltributyltin, and 0.1 mmol of Pd(PPh3)4 in 4 mL DMF was stirred and heated at 90° C. for 1-16 h. Chromatography provided ethyl 3-vinylphenylacetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05731432 |
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| Source dataset | uspto-grants-1998_03 |
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| ORD ID | ord-22f4a8336221412198601584d84cd4b1 |
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| Source note | uspto-grants-1998_03 |
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